HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86623848, compound → HCID 67361455, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86623848 | HCID 86623848 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 67361455 | HCID 67361455 | — |
Reaction Steps
) The title compound was prepared from the above described {2-[3-(3-bromo-phenyl)-3-oxo-propionylamino]-5-ethoxy-4-trifluoromethyl-phenyl}-carbamic acid tert-butyl ester (1.459 g, 2.675 mmol) and TFA (10 mL) according to general procedure I step 2. Obtained as a light yellow solid (0.940 g, 82%). MS (ISP) 427.1 [(M+H)+] and 429.1 [(M+2+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07511033B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-5440bf8de9da4754ab76a2702ef7c71b |
| Source note | uspto-grants-2009_03 |