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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1787421Generated: October 28, 2026

Trifluoroacetic acid → HCID 67361924, compound

https://huagongshe.com/reaction/1787421

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 86623850HCID 86623850—
SolventDichloromethaneHCID 6344—
ProductHCID 67361924HCID 67361924—

Reaction Steps

) The title compound was prepared from the above described {2-[3-(3-bromo-phenyl)-3-oxo-propionylamino]-5-dimethylamino-4-trifluoromethyl-phenyl}-carbamic acid tert-butyl ester (2.2 g, 4.04 mmol) and TFA (15 mL) in DCM (45 mL) according to general procedure I step 2. Obtained as an off-white solid (1.61 g, 93%). MS (ISP) 426.0 [(M+H)+]; mp 193° C. (dec).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07511033B2
Source datasetuspto-grants-2009_03
ORD IDord-bafa2403e8f54a4599e4d11dcb8b0ccb
Source noteuspto-grants-2009_03