HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 67361924, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86623850 | HCID 86623850 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67361924 | HCID 67361924 | — |
Reaction Steps
) The title compound was prepared from the above described {2-[3-(3-bromo-phenyl)-3-oxo-propionylamino]-5-dimethylamino-4-trifluoromethyl-phenyl}-carbamic acid tert-butyl ester (2.2 g, 4.04 mmol) and TFA (15 mL) in DCM (45 mL) according to general procedure I step 2. Obtained as an off-white solid (1.61 g, 93%). MS (ISP) 426.0 [(M+H)+]; mp 193° C. (dec).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07511033B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-bafa2403e8f54a4599e4d11dcb8b0ccb |
| Source note | uspto-grants-2009_03 |