HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10003096, compound → HCID 9979591, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10003096 | HCID 10003096 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | HCID 9979591 | HCID 9979591 | 24% |
Reaction Steps
In a procedure analogous to example 46, reaction of N-[1-(6-{[(1S)-1-phenylethyl]amino}pyrazin-2-yl)-1H-benzimidazol-5-yl]nicotinamide (33 mg, 0.10 mmol) with LiAlH4 (5.7 mg 0.15 mmol) furnished the product (10 mg, 24%) after chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07511047B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-2681eac091f24b6d9eb0646017251629 |
| Source note | uspto-grants-2009_03 |