HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Iodobenzoic acid → HCID 22058256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Iodobenzoic acid | HCID 6941 | — |
| Reactant | 3-Ethoxyaniline | HCID 12120 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Catalyst | Copper | HCID 23978 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22058256 | HCID 22058256 | — |
Reaction Steps
m-Phenetidine (5 ml, 38.7 mmol) is added to a solution of KOH (7.385 g, 131.6 mmol), water (77 ml) and 2-iodobenzoic acid (9.6 g, 38.7 mmol). Powdered copper (77 mg, 1.22 μmol) is added and the mixture is refluxed under stirring over night (16 h).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07511064B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-98b2c4adc68c4744a60a514a1cbaff45 |
| Source note | uspto-grants-2009_03 |