Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | 3-Pentyl-2-thioxo-1,2,3,7-tetrahydro-6H-purin-6-one | HCID 57600236 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178446164 | HCID 178446164 | 79.4% |
Reaction Steps
3-Pentyl-2-thioxo-1,2,3,7-tetrahydro-6H-purin-6-one (6.0 g, 16 mmol) was mixed with hydrazine (10 mL, 300 mmol) and water (10 mL). The mixture was heated at 100° C. for 8 h. The solid formed was filtered and washed with water to give the desired product (3.0 g, 78%). LCMS calculated for C10H17N6O (M+H): 237.1; found: 237.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07511050B2 |
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| Source dataset | uspto-grants-2009_03 |
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| ORD ID | ord-c5affaf43c70471d821746c1e957c5ee |
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| Source note | uspto-grants-2009_03 |
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