Isobutyric Acid → HCID 21900164, compound

HRID 1788257Notes

Reaction equation

HRID 1788257 reaction equation
[OH-].[CH2:2]([N+:6]([CH2:15][CH2:16][CH2:17][CH3:18])([CH2:11][CH2:12][CH2:13][CH3:14])[CH2:7][CH2:8][CH2:9][CH3:10])[CH2:3][CH2:4][CH3:5].[C:19]([OH:24])(=[O:23])[CH:20]([CH3:22])[CH3:21]>O>[C:19]([O-:24])(=[O:23])[CH:20]([CH3:22])[CH3:21].[CH2:15]([N+:6]([CH2:2][CH2:3][CH2:4][CH3:5])([CH2:7][CH2:8][CH2:9][CH3:10])[CH2:11][CH2:12][CH2:13][CH3:14])[CH2:16][CH2:17][CH3:18]

Participants

4

Reactant 2

HCID 6590Isobutyric AcidHCID 2723671Tetrabutylammonium Hydroxide

Product 1

HCID 21900164HCID 21900164, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A 40 wt % solution of tetrabutylammonium hydroxide in water (250 mL, 99 g, 382 mmol), water (300 mL) and isobutyric acid (33.8 g, 382 mmol) was stirred at ambient temperature for 30 min. The solvent was removed in vacuo to afford the title compound (5) as a waxy solid, which was used without further purification.

Workup

  1. customThe solvent was removed in vacuo

Sources & evidence

ORD record
ord-78195199e32d4abaa861ba5154e7b4ae
Source dataset
uspto-grants-2009_03
Patent number
US07511158B2

Reaction notes

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