HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 21900164, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Isobutyric Acid | HCID 6590 | — |
| Reactant | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| Product | HCID 21900164 | HCID 21900164 | — |
Reaction Steps
Alternatively, a 1M solution of tetrabutylammonium hydroxide in methanol (1 L, 1 mol) and isobutyric acid (88.5 g, 1 mol) was stirred at ambient temperature for 30 min. The solvent was removed in vacuo to afford the title compound (5) as a waxy solid, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07511158B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-55b291c8e2044046a869b5ae58a39430 |
| Source note | uspto-grants-2009_03 |