Ammonium Hydroxide → HCID 178512964, compound

HRID 1788303Notes

Reaction equation

HRID 1788303 reaction equation
[NH2:1][C@H:2]([C:10]([OH:12])=[O:11])[CH2:3][CH2:4][CH2:5][NH:6][C:7](=[NH:9])[NH2:8].[OH-].[NH4+:14]>O>[NH2:1][CH:2]([CH2:3][CH2:4][CH2:5][NH:6][C:7]([NH2:9])=[NH:8])[C:10]([O-:12])=[O:11].[NH4+:14]

Participants

4

Reactant 2

HCID 14923Ammonium HydroxideHCID 178418600HCID 178418600, compound

Product 1

HCID 178512964HCID 178512964, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Separately, in a single-necked, round bottomed flask, equipped with a magnetic stirrer, 10.45 g (60 mmol) of Arginine is dissolved in 300 ml of water. To this is added 78 ml of 1M ammonium hydroxide with vigorous stirring, until heat production ceases. At this point the water is removed by evaporation to yield the carboxylate salt, ammonium 2-amino-5-guanidinopentanoate, shown below.

Workup

  1. customSeparately, in a single-necked, round bottomed flask, equipped with a magnetic stirrer
  2. temperatureuntil heat production ceases
  3. customAt this point the water is removed by evaporation

Sources & evidence

ORD record
ord-deb832ac8bfe4632baf579b126449788
Source dataset
uspto-grants-2009_03
Patent number
US07511162B2

Reaction notes

Loading…