HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyclohexylamino-3-[(3-phenyl-quinoxaline-6-carbonyl)-amino]-benzoic Acid Ethyl Ester → HCID 57602929, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyclohexylamino-3-[(3-phenyl-quinoxaline-6-carbonyl)-amino]-benzoic Acid Ethyl Ester | HCID 57603019 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 57602929 | HCID 57602929 | — |
Reaction Steps
Compound 41 (0.95 mmol) from the previous step was refluxed in 80 mL acetic acid for 3.5 h. The mixture was then evaporated to dryness and dried overnight under high vacuum to yield Compound 42 in quantitative yield. It was not further purified before saponification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07511145B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-d7044bea1cd14d9da16f302f9bea6c67 |
| Source note | uspto-grants-2009_03 |