HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 5275977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 5276026 | HCID 5276026 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 5275977 | HCID 5275977 | 17% |
Reaction Steps
Following the same reaction procedure and workup as for Compound 405, 450 mg (0.9 mmol) of the product from the previous step was cyclized with 40 mL acetic acid and saponified with 35 mL EtOH and 7 mL 1M NaOH to produce 70 mg (17% yield) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07511145B2 |
| Source dataset | uspto-grants-2009_03 |
| ORD ID | ord-7b5b89fcdf564fe386e02f5424db8de5 |
| Source note | uspto-grants-2009_03 |