HRID1788469

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID65746

1-Naphthalenol, 5-amino-

C10H9NO

结构：O=C(NN1CCOCC1)c1ccc2c(c1)nc(-c1ccc3nc(-c4ccccc4)cnc3c1)n2C1CCCCC1

HCID57603045

未命名化合物

PRODUCTS

生成物

结构：O=C(Nc1cccc2c(O)cccc12)c1ccc2c(c1)nc(-c1ccc3nc(-c4ccccc4)cnc3c1)n2C1CCCCC1

HCID136096456

未命名化合物

收率 25%

PROCEDURE

实验过程

The general procedure described for Compound 574 was used with 5-amino-naphthalen-1-ol (15.9 mg), producing 7 mg of the title compound (25% yield). MS: 590.24 (M+H+) HPLC Procedure A, retention time=15.26 min.

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-6d15d8fd54c041dc9ea09e3f50429660
来源数据集: uspto-grants-2009_03
DOI: 10.6084/m9.figshare.5104873.v1
专利: US07511145B2
来源说明: uspto-grants-2009_03

反应 SMILES

N1(N[C:8]([C:10]2[CH:40]=[CH:39][C:13]3[N:14]([CH:33]4[CH2:38][CH2:37][CH2:36][CH2:35][CH2:34]4)[C:15]([C:17]4[CH:18]=[C:19]5[C:24](=[CH:25][CH:26]=4)[N:23]=[C:22]([C:27]4[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=4)[CH:21]=[N:20]5)=[N:16][C:12]=3[CH:11]=2)=[O:9])CCOCC1.[NH2:41][C:42]1[CH:51]=[CH:50][CH:49]=[C:48]2[C:43]=1[CH:44]=[CH:45][CH:46]=[C:47]2[OH:52]>>[OH:52][C:47]1[CH:46]=[CH:45][CH:44]=[C:43]2[C:48]=1[CH:49]=[CH:50][CH:51]=[C:42]2[NH:41][C:8]([C:10]1[CH:40]=[CH:39][C:13]2[N:14]([CH:33]3[CH2:38][CH2:37][CH2:36][CH2:35][CH2:34]3)[C:15]([C:17]3[CH:18]=[C:19]4[C:24](=[CH:25][CH:26]=3)[N:23]=[C:22]([C:27]3[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=3)[CH:21]=[N:20]4)=[N:16][C:12]=2[CH:11]=1)=[O:9]