Hydrochloric Acid → HCID 13118258, compound

HRID 1788836Notes

Reaction equation

HRID 1788836 reaction equation
[O:1]=[C:2]1[N:8]2[CH:4]([S:5][C:6]([O:12][C:13]3[CH:18]=[CH:17][C:16]([CH3:19])=[CH:15][CH:14]=3)=[C:7]2[C:9]([O-:11])=[O:10])[CH2:3]1.[Na+].Cl>>[O:1]=[C:2]1[N:8]2[CH:4]([S:5][C:6]([O:12][C:13]3[CH:18]=[CH:17][C:16]([CH3:19])=[CH:15][CH:14]=3)=[C:7]2[C:9]([OH:11])=[O:10])[CH2:3]1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 23683695HCID 23683695, compound

Product 1

HCID 13118258HCID 13118258, compoundYield 48.2%

Procedure

An aqueous solution of 32 mg of sodium 7-oxo-3-(4-tolyloxy)-4-thia-1-azabicyclo[3,2,0]hept-2-ene-2-carboxylate was acidified to pH 2.0 with dilute hydrochloric acid, and was then extracted with ethyl acetate. The organic layer was backwashed with water, and then dried and evaporated in vacuo to afford 14.3 mg of the above acid as a solid.

Workup

  1. extractionwas then extracted with ethyl acetate
  2. customdried
  3. customevaporated in vacuo

Sources & evidence

ORD record
ord-6d313810f4dd42a88f65f7287dd25216
Source dataset
uspto-grants-1987_08
Patent number
US04684640

Reaction notes

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