HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 13821868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 13821832 | HCID 13821832 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13821868 | HCID 13821868 | 84.2% |
Reaction Steps
Methyliodide (1.7 g) was added dropwise to a solution of 8-chloro-3-dimethylaminomethyl-2-methylimidazo[2,1-a]isoquinoline (2.8 g) in ethanol (34 ml) at room temperature and the mixture was stirred for 14 hours. The resulting precipitate was collected by filtration, washed with ethanol and dried in a desiccator to give 8-chloro-2-methyl-3-trimethylammoniomethylimidazo[2,1-a]isoquinoline iodide (3.58 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04686227 |
| Source dataset | uspto-grants-1987_08 |
| ORD ID | ord-93256b0b1b2d4e259b6a55c562dc49d1 |
| Source note | uspto-grants-1987_08 |