HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1789079Generated: October 30, 2026
HCID 13912878, compound → HCID 13912880, compound
https://huagongshe.com/reaction/1789079
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 13912878 | HCID 13912878 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13912880 | HCID 13912880 | — |
Reaction Steps
A suspension of 3.04 g of 5-amino-2-methoxy-4-nitrobenzamide and 110 mg of 10 % palladium carbon in 300 ml of methanol was stirred at 60° C. under a hydrogen atmosphere. After absorption of hydrogen was completed, the catalyst was removed by filtration, and the filtrate was concentrated to give the title compound, m.p. 181°-183° C., yield of 2.18 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04686292 |
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| Source dataset | uspto-grants-1987_08 |
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| ORD ID | ord-491a4f8f742343318b3697e3cf01bfb4 |
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| Source note | uspto-grants-1987_08 |
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