HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfoxide → HCID 13768078, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 13768083 | HCID 13768083 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 13768078 | HCID 13768078 | 93.1% |
Reaction Steps
6.0 g of 2-[2-(4-phenylpiperazin-1-yl)ethylthio]benzylalcohol, 2.60 g of oxalyl chloride, 3.2 g of dimethylsulfoxide and 9.3 g of triethylamine are treated in the same manner as described above. 5.55 g of 2-[2-(4-phenylpiperazin-1-yl)ethylthio]benzaldehyde are obtained. Yield: 93%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04689327 |
| Source dataset | uspto-grants-1987_08 |
| ORD ID | ord-eb12f920bec740a89ef3f6602f83b842 |
| Source note | uspto-grants-1987_08 |