HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 53651586, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 18609505 | HCID 18609505 | — |
| Product | HCID 53651586 | HCID 53651586 | — |
Reaction Steps
cis-2,3-Dihydro-1-methyl-1H-indene-2-carboxylic acid (52.6 g) is converted to its acid chloride by treatment with thionyl chloride (130 ml). Excess thionyl chloride is distilled off and the acid chloride is distilled, b.p. 86°-89° C./0.45 mmHg. The yield is 47.9 g, 83%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04689339 |
| Source dataset | uspto-grants-1987_08 |
| ORD ID | ord-5a05f21af04347eba8fca34c13fc77a3 |
| Source note | uspto-grants-1987_08 |