HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 54146119, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 53651586 | HCID 53651586 | — |
| Product | HCID 54146119 | HCID 54146119 | 92% |
Reaction Steps
cis-1-(2,3-Dihydro-1-methyl-1H-inden-2-yl)ethanone is prepared by the treatment of cis-2,3-dihydro-1-methyl-1H-indene-2-carboxylic acid chloride with ethoxymagnesiummalonic acid ethyl ester in dry ether and thereafter by the treatment of sulfuric acid according to the publication (Reynolds G. A. and Hauser, C. B., Org. Synth. 30 (1957) 70). The yield is 92%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04689339 |
| Source dataset | uspto-grants-1987_08 |
| ORD ID | ord-0c8bd1726a624b558cf9760fcb686e24 |
| Source note | uspto-grants-1987_08 |