HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 13649405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 15338833 | HCID 15338833 | — |
| Reactant | HCID 15588516 | HCID 15588516 | — |
| Product | HCID 13649405 | HCID 13649405 | 59% |
Reaction Steps
The 1,6-dimethyl-indene-2-carboxylic acid can be prepared by the treatment of α-acetyl-4-methylbenzenepropanoic acid ethyl ester with sulfuric acid (Shadbolt, R. S., J. Chem. Soc. (C), (1970) 920). Recrystallization from ethanol, m.p. 174°-182° C. Yield 59%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04689339 |
| Source dataset | uspto-grants-1987_08 |
| ORD ID | ord-7ea4f8fc554c4262acbd33d788d8a118 |
| Source note | uspto-grants-1987_08 |