HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 15338836, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 20188240 | HCID 20188240 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 15338836 | HCID 15338836 | 59.5% |
Reaction Steps
Bromine (2.80 g) is added to 1-(3,5-dimethyl-inden-2-yl)ethanone (3.00 g) in dry ether (30 ml), while keeping the temperature at +10° C. The mixture is extracted with water, several times with the diluted NaHCO3 solution, again with water, dried and evaporated under reduced pressure to afford the product (2.54 g, 59%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04689339 |
| Source dataset | uspto-grants-1987_08 |
| ORD ID | ord-87ac3ca1a6a44205a81100de76b418af |
| Source note | uspto-grants-1987_08 |