HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 13649411, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-methyl-2,3-dihydro-1H-indene-2-carboxylic acid | HCID 15338842 | — |
| Product | HCID 13649411 | HCID 13649411 | — |
Reaction Steps
A stirred mixture of 2,3-dihydro-2-methyl-1H-indene-2-carboxylic acid (6.70 g) and thionyl chloride (70 ml) is heated under reflux for 14 hr. The ecess of thionyl chloride is removed and the acid chloride is distilled. Yield 5.35 g, 72%, bp. 93°-98° C./3 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04689339 |
| Source dataset | uspto-grants-1987_08 |
| ORD ID | ord-1b094d5a56494e2da452893b6b974dbc |
| Source note | uspto-grants-1987_08 |