HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → 2-Bromo-1-(2,3-dihydro-2-methyl-1h-inden-2-yl)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 15338843 | HCID 15338843 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Bromo-1-(2,3-dihydro-2-methyl-1h-inden-2-yl)ethanone | HCID 15338844 | — |
Reaction Steps
1-(2,3-Dihydro-2-methyl-1H-inden-2-yl)ethanone (3.69 g) in methylene chloride (40 ml) is stirred and cooled at 10° C. during the dropwise addition of bromine (2.82 g)/methylene chloride (10 ml). Work-up of the resultant solution gives 2-bromo-1-(2,3-dihydro-2-methyl-1H-inden-2-yl)ethanone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04689339 |
| Source dataset | uspto-grants-1987_08 |
| ORD ID | ord-85a2fa7645354306a0bcb4aae40fe67f |
| Source note | uspto-grants-1987_08 |