HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Ethyl (2S)-2-amino-4-phenylbutanoate--hydrogen chloride (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | (S)-2-amino-4-phenylbutanoic acid | HCID 2724505 | — |
| Product | Ethyl (2S)-2-amino-4-phenylbutanoate--hydrogen chloride (1/1) | HCID 2734606 | — |
Reaction Steps
Hydrogen chloride gas is bubbled through a solution of (L)-homophenylalanine (5.13 g, 28.7 mmol) in 100 mL of ethanol for 5 minutes. The mixture is stirred at room temperature for 16 hours. The mixture is concentrated in vacuo to yield L-homophenylalanine ethyl ester hydrochloride as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071169B2 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-9c82313f2b26441a97fe05b17f01ced8 |
| Source note | uspto-grants-2006_07 |