2,3-Dichloroquinoxaline → HCID 22036340, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in Example 1, Step 1, starting from 2-phenoxyethanol (3.7 g, 26.8 mmol), 2,3-dichloroquinoxaline (1.33 g, 6.7 mmol) and KO-t-Bu (0.75 g, 6.7 mmol): yield 0.74 g (37%); mp 99.5-101.5° C., HRMS m/z calcd for C16H13CIN2O2(M)+300.0666, found 300.0672. Anal. (C16H13CIN2O2) C, H, N.

Provenance & Evidence