HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131725826, compound → HCID 9881344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131725826 | HCID 131725826 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | HCID 9881344 | HCID 9881344 | 80.2% |
Reaction Steps
A solution of 2-Mercaptomethyl-3-piperidin-4-yl-propionic acid TFA salt (0.1 g, 0.32 mmol) in acetic anhydride (2 mL) was stirred over night under argon and then concentrated under reduced pressure. Purification by HPLC (10→50% acetonitrile, 0.1% TFA in water) gave the title compound (63 mg, 80%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071175B1 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-65be9be147ec4d6cba76109aff30097f |
| Source note | uspto-grants-2006_07 |