HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54210448, compound → HCID 9837241, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54210448 | HCID 54210448 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 9837241 | HCID 9837241 | 126.1% |
Reaction Steps
2-Acetylsulfanylmethyl-3-(6-tert-butoxycarbonylamino-pyridin-3-yl)-propionic acid ethyl ester (38 mg, 0.096 mmol) was dissolved in conc. HCl (2.0 mL) under argon. The solution was stirred at room temperature for 1 h and then heated to reflux for 1 h. Concentration under reduced pressure gave the title compound (25.7 mg, 100%) as the hydrochloride salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071175B1 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-c422c5c80ac74dc8a85345718451f205 |
| Source note | uspto-grants-2006_07 |