HRID1789810

反应详情

EQUATION

反应方程式

HRID 1789810 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2-Acetylsulfanylmethyl-3-(6-tert-butoxycarbonylamino-pyridin-3-yl)-propionic acid ethyl ester (38 mg, 0.096 mmol) was dissolved in conc. HCl (2.0 mL) under argon. The solution was stirred at room temperature for 1 h and then heated to reflux for 1 h. Concentration under reduced pressure gave the title compound (25.7 mg, 100%) as the hydrochloride salt.

WORKUP

后处理

  1. temperatureheated
  2. temperatureto reflux for 1 h
  3. concentrationConcentration under reduced pressure