HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53958532, compound → HCID 10130758, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53958532 | HCID 53958532 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 10130758 | HCID 10130758 | — |
Reaction Steps
2-Acetylsulfanylmethyl-3-(6-tert-butoxycarbonylamino-pyridin-3-yl)-2-methyl-propionic acid tert-butyl ester (4 mg, 9.4 μmol) was dissolved in conc. HCl under argon. The solution was heated to reflux for 1 h. Concentration under reduced pressure yielded the title compound as the hydrochloride salt (2.5 mg, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071175B1 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-e888b47742fc4305b15e5deb0b2c9806 |
| Source note | uspto-grants-2006_07 |