HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54067761, compound → HCID 9794764, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54067761 | HCID 54067761 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 9794764 | HCID 9794764 | — |
Reaction Steps
2-Acetylsulfanylmethyl-2-(6-tert-butoxycarbonylamino-pyridin-3-ylmethyl)-butyric acid ethyl ester (12.3 mg, 30 μmol) was dissolved in conc. HCl (2 mL) under argon. The solution was heated to reflux for 24 h. Concentration under reduced pressure gave the title compound as the hydrochloride salt (8.3 mg, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071175B1 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-cfa2598c674d45cd8384f953ab1e1107 |
| Source note | uspto-grants-2006_07 |