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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1789871Generated: October 29, 2026

Trifluoroacetic acid → HCID 86760119, compound

https://huagongshe.com/reaction/1789871

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 54460231HCID 54460231—
SolventDichloromethaneHCID 6344—
ProductHCID 86760119HCID 86760119132%

Reaction Steps

TFA (1.5 mL) was added to a solution of 2-acetylsulfanylmethyl-3-(2-[N,N-bis(tert-butoxycarbonyl)amino]-pyrimidin-5-yl)-propionic acid ethyl ester (225 mg, 0.46 mmol) in methylene chloride (1.5 mL). The reaction was stirred for 120 min and concentrated under reduced pressure to give the title compound (172 mg, 94%) as the TFA salt.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07071175B1
Source datasetuspto-grants-2006_07
ORD IDord-2ddc12cb8a4744238f5c2c85ca990667
Source noteuspto-grants-2006_07