HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54201262, compound → HCID 22036122, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54201262 | HCID 54201262 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 22036122 | HCID 22036122 | — |
Reaction Steps
A solution of 3-acetylsulfanyl-2-(6-tert-butoxycarbonylamino-pyridin-3-ylmethyl)-pentanoic acid ethyl ester/B (51.6 mg; 0.13 mmol) in concentrated HCl (2 mL) was refluxed under argon for 1.5 hours. The reaction mixture was allowed to cool to room temperature and concentrated under reduced pressure to afford 34.7 mg of the title compound as the hydrochloride salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071175B1 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-7acc4118a688498fb1276bc4af28fcef |
| Source note | uspto-grants-2006_07 |