HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54294565, compound → HCID 22036157, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54294565 | HCID 54294565 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 22036157 | HCID 22036157 | 110.5% |
Reaction Steps
A solution of 2-acetylsulfanylmethyl-3-(6-tert-butoxycarbonylamino-5-chloro-pyridin-3-yl)-propionic acid ethyl ester (55mg, 0.132 mmol) in concentrated HCl (4 mL) was refluxed for 90 min. The reaction was cooled and concentrated under reduced pressure to give the title compound as the HCl salt (36mg, 96.4%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071175B1 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-2a9d04f03e0041fab320d6b1e0866204 |
| Source note | uspto-grants-2006_07 |