Hydrochloric Acid → HCID 22036012, compound

Participants

Reaction Steps

Hydrochloric acid (38%, 4 mL) was added to 2-acetylsulfanylmethyl-3-(6-tert-butoxycarbonylamino-pyridin-3-yl)-pentanoic acid ethyl ester (0.041 g, 0.1 mmol) under argon and the mixture was heated to reflux for 4 h. Concentration under reduced pressure and drying (45° C., 0.3 mbar) afforded the title compound as the hydrochloride salt (0.027 mg, 97%).

Provenance & Evidence