HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53756755, compound → HCID 22036108, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53756755 | HCID 53756755 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 22036108 | HCID 22036108 | — |
Reaction Steps
2-Acetylsulfanylmethyl-3-(6-tert-butoxycarbonylamino-pyridin-3-yl)4-phenyl-butyric acid ethyl ester (0.14 g, 0.3 mmol) was dissolved in conc. HCl (5.0 mL). The solution was heated to reflux for 4.5 h under argon. Concentration under reduced pressure gave the title compound as the hydrochloride salt (100 mg, 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071175B1 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-1cfb6a7fe4ee45cf909ed85a4f33fcad |
| Source note | uspto-grants-2006_07 |