HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53847096, compound → HCID 22036151, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53847096 | HCID 53847096 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 22036151 | HCID 22036151 | — |
Reaction Steps
2-Acetylsulfanylmethyl-3-[6-(2,2-dimethyl-propionylamino)-pyridin-3-yl]-hexanoic acid ethyl ester (40.4 mg, 99 μmol) was dissolved under argon in aqueous hydrochloric acid (37%, 4.2 mL) and heated under reflux for 2 h. Concentration under reduced pressure (0.3 torr, 40° C.) gave the title compound as the hydrochloride salt (28 mg, 97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071175B1 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-2fe91ed6f0d34deca63adedf15b027ff |
| Source note | uspto-grants-2006_07 |