HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → 3-Pyridineethanol,6-methoxy-(9CI)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 5-Bromo-2-methoxypyridine | HCID 2734895 | — |
| Product | 3-Pyridineethanol,6-methoxy-(9CI) | HCID 22038367 | 62.7% |
Reaction Steps
5-Bromo-2-methoxypyridine (2.628 g) synthesized as reported in Tetrahedron, 1373 (1985). was dissolved in diethyl ether (40 ml) and then treated as in the above Production Example 16-1 to give the title compound (1.342 g) as a pale yellow oil (yield: 62.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071201B2 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-2f1de5f6f73f47e19d07246a745e2b19 |
| Source note | uspto-grants-2006_07 |