HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → 1-[1-(4-Methanesulfonylaminomethylphenethyl)piperidin-4-yl]indoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 1-[1-(4-Aminomethylphenethyl)piperidin-4-yl]indoline | HCID 22038221 | — |
| Product | 1-[1-(4-Methanesulfonylaminomethylphenethyl)piperidin-4-yl]indoline | HCID 22038049 | 54.5% |
Reaction Steps
1-[1-(4-Aminomethylphenethyl)piperidin-4-yl]indoline (0.120 g) and methanesulfonyl chloride (0.030 ml) were treated as in Example 36 to give the title compound (0.078 g) as a pale yel low oil (yield: 54.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071201B2 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-61788ba822c24d7a88900203c3ff9301 |
| Source note | uspto-grants-2006_07 |