HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22042415, compound → 2-(1-Ethylcyclopropyl)-2-methyl-1,3-dioxolan
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22042415 | HCID 22042415 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-(1-Ethylcyclopropyl)-2-methyl-1,3-dioxolan | HCID 22042443 | 78.6% |
Reaction Steps
500 mg of olefin 8 is dissolved in 15 ml of ethyl acetate, 150 mg of platinum(IV) oxide is added and hydrogenated in a hydrogenating apparatus until no more hydrogen is taken up. After filtration, it is concentrated by evaporation, whereby 398 mg of title compound 195 is obtained as a colorless oil, which is immediately further reacted.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071344B1 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-8f2172af70fa4b9d89d9973bf5fff44b |
| Source note | uspto-grants-2006_07 |