HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22041793, compound → HCID 9962545, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22041793 | HCID 22041793 | — |
| Reactant | HCID 22041814 | HCID 22041814 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 9962545 | HCID 9962545 | 82.2% |
Reaction Steps
To 3.0 g (7.68 mmol) of compound 134 was added a solution of 4.0 g (9.24 mmol) of compound 135 in 200 mL of dichloromethane. The reaction was allowed to stir at ambient temperature for 48 hours. The fine, white solid was collected to give 5.2 g of compound 157.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07071231B2 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-de621f935b8f431f98196f90fe51bfa6 |
| Source note | uspto-grants-2006_07 |