HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Nitrobenzylamino)succinic acid dimethyl ester → HCID 23535553, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Nitrobenzylamino)succinic acid dimethyl ester | HCID 23535554 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23535553 | HCID 23535553 | — |
Reaction Steps
A mixture of 2-(2-nitrobenzylamino)succinic acid dimethyl ester [from a) above] (7.6 g, 25.65 mmol) and platinum oxide (349.51 mg, 1.54 mmol) was shaken in methanol on a Parr hydrogenation apparatus under 50 psi of hydrogen gas. After 12 h the mixture was filtered and concentrated to give 6.6 g of the title compound as a light brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07074783B2 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-23085d74e8b84ffc85b6cd273237a8e0 |
| Source note | uspto-grants-2006_07 |