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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1791885Generated: November 3, 2026

HCID 69111912, compound → HCID 69111274, compound

https://huagongshe.com/reaction/1791885

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69111912HCID 69111912—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 69111274HCID 69111274—

Reaction Steps

A mixture of 5-(2-nitro-phenylsulfanyl)-2-propionylamino-benzoic acid methyl ester (110 mg, 0.31 mmol, prepared according to Sevbo et al. 1976) and palladium-on-charcoal (10%, 25 mg) in ethyl acetate (5 mL) was stirred in an atmosphere of hydrogen (1 atm) at room temperature for 2 hours. The catalyst was filtered off and the solvent was removed by evaporation to yield the title compound quantitatively.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07074831B2
Source datasetuspto-grants-2006_07
ORD IDord-c4624dff17464e99b1a38f46df62301a
Source noteuspto-grants-2006_07