HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69111912, compound → HCID 69111274, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69111912 | HCID 69111912 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 69111274 | HCID 69111274 | — |
Reaction Steps
A mixture of 5-(2-nitro-phenylsulfanyl)-2-propionylamino-benzoic acid methyl ester (110 mg, 0.31 mmol, prepared according to Sevbo et al. 1976) and palladium-on-charcoal (10%, 25 mg) in ethyl acetate (5 mL) was stirred in an atmosphere of hydrogen (1 atm) at room temperature for 2 hours. The catalyst was filtered off and the solvent was removed by evaporation to yield the title compound quantitatively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07074831B2 |
| Source dataset | uspto-grants-2006_07 |
| ORD ID | ord-c4624dff17464e99b1a38f46df62301a |
| Source note | uspto-grants-2006_07 |