HRID1792023

反应详情

EQUATION

反应方程式

HRID 1792023 的结构方程式

PROCEDURE

实验过程

4-[7-(2-Methoxyphenyl)-1-(carboxymethyl)-3-methyl-2,6-dioxo-2,3,6,7-tetrahydro-1H-purin-8-yl]piperazine-1-carboxylic acid tert-butyl ester (3 mg) was dissolved in trifluoroacetic acid (0.5 ml), and the reaction mixture was stirred at room temperature for 30 minutes. After the solvent was removed, the residue was purified by reversed phase high performance liquid chromatography to give 4.14 mg of the title compound.

WORKUP

后处理

  1. customAfter the solvent was removed
  2. customthe residue was purified by reversed phase high performance liquid chromatography