HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1792034Generated: November 4, 2026
Trifluoroacetic acid → HCID 22029891, compound
https://huagongshe.com/reaction/1792034
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 1H-Purine-2,6-dione, 3,7-dihydro-8-chloro-7-(2-chlorophenyl)-1,3-dimethyl- | HCID 3055772 | — |
| Product | HCID 22029891 | HCID 22029891 | — |
Reaction Steps
2,5-(Diaza-bicyclo[2.2.1]heptane)-2-carboxylic acid tert-butyl ester (50 mg) and 8-chloro-7-(2-chlorophenyl)-1,3-dimethyl-3,7-dihydropurine-2,6-dione (10 mg) were mixed, and the mixture was stirred at 150° C. for 3 hours. The residue was dissolved in trifluoroacetic acid, and the solution was concentrated. The residue was purified by reversed phase high performance liquid chromatography to give 5.10 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07074798B2 |
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| Source dataset | uspto-grants-2006_07 |
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| ORD ID | ord-1f9c3b3406294c98a9964679f62bb457 |
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| Source note | uspto-grants-2006_07 |
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