HCID 16120412, compound → HCID 16120413, compound

Participants

Reaction Steps

2,2-Dimethylpropionic acid 7-benzyl-3-methyl-2,6-dioxo-2,3,6,7-tetrahydropurin-1-ylmethyl ester (4.26 g) was dissolved in acetic acid (100 ml), and 10% palladium on carbon (1.5 g) was added thereto. The reaction mixture was stirred under hydrogen atmosphere at room temperature overnight, filtered through Celite, and the filtrate was concentrated to give 2.98 g of the title compound.

Provenance & Evidence