Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalyl chloride → 2,4-Dichlorobenzoyl isocyanate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | 2,4-Dichlorobenzamide | HCID 75556 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 2,4-Dichlorobenzoyl isocyanate | HCID 11629887 | — |
반응 단계
2,4-Dichlorobenzamide was dissolved in dichloromethane, after which 1.5 eq. of oxalyl chloride were added and the mixture was heated to reflux for 16 hours. The reaction mixture was then concentrated under high vacuum and reacted in step b without any further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07078404B2 |
| 출처 데이터셋 | uspto-grants-2006_07 |
| ORD ID | ord-da622c2e851144e18b5e32b81f602c38 |
| 출처 메모 | uspto-grants-2006_07 |