反应详情

2,4-Dichlorobenzamide was dissolved in dichloromethane, after which 1.5 eq. of oxalyl chloride were added and the mixture was heated to reflux for 16 hours. The reaction mixture was then concentrated under high vacuum and reacted in step b without any further purification.

1. temperaturethe mixture was heated
2. temperatureto reflux for 16 hours
3. concentrationThe reaction mixture was then concentrated under high vacuum
4. customreacted in step b without any further purification