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HRID1793527

反应详情

EQUATION

反应方程式

HRID 1793527 的结构方程式

REACTANTS

反应物

2
结构：OB(O)c1ccccc1
HCID66827

Boronic acid, phenyl-

C6H7BO2

结构：CC(C)(C)OC(=O)N1CC[C@H]2[C@@H](C1)c1cc(Br)cc3c1N2CC3
HCID20577007

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CC[C@H]2[C@@H](C1)c1cc(-c3ccccc3)cc3c1N2CC3
HCID11740272

未命名化合物

PROCEDURE

实验过程

The title compound was prepared by the method of Example 89 step C from tert-butyl(6aS,10aR)-2-bromo-4,5,7,8,10,10a-hexahydropyrido[4,3-b]pyrrolo[3,2,1-hi]indole-9(6aH)carboxylate (189 mg, 0.5 mmol) and phenylboronic acid (122 mg, 1.0 mmol) to afford after chromatographic purification the title compound (74 mg, 20%).

WORKUP

后处理

  1. customto afford
  2. customafter chromatographic purification the title compound (74 mg, 20%)