Ethyl vinyl ether → (2-(Ethenyloxy)ethyl)cyclohexane

HRID 1793767Notes

Reaction equation

HRID 1793767 reaction equation
[CH:1]1([CH2:7][CH2:8][OH:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[CH:10](OCC)=[CH2:11]>C([O-])(=O)C.[Hg+]>[CH:10]([O:9][CH2:8][CH2:7][CH:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1)=[CH2:11]

Participants

4

Reactant 2

HCID 8023Ethyl vinyl etherHCID 205082-Cyclohexylethanol

Product 1

HCID 21363356(2-(Ethenyloxy)ethyl)cyclohexane

Reagents, catalysts & solvents 1

HCID 61181Mercurous acetateCatalyst

Procedure

Cyclohexylethyl alcohol was mixed with ethyl vinyl ether. Mercury acetate was added thereto and this mixture was stirred at room temperature for 12 hours. The resultant reaction mixture was extracted with ethyl acetate and water, and the extract was washed with water and then distilled under reduced pressure to obtain cyclohexylethyl vinyl ether (X-1) as the target compound.

Workup

  1. customThe resultant reaction mixture
  2. extractionwas extracted with ethyl acetate and water
  3. washthe extract was washed with water
  4. distillationdistilled under reduced pressure

Sources & evidence

ORD record
ord-e3da1ad9914a4f978033cb83e4daf5c9
Source dataset
uspto-grants-2006_04
Patent number
US07022456B2

Reaction notes

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