HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86595211, compound → HCID 86595210, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86595211 | HCID 86595211 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86595210 | HCID 86595210 | 98.7% |
Reaction Steps
To a solution of 92 mg of tert-butyl [2-(4-isopropyl-2-nitrophenyl)ethyl]carbamate in 2 mL of ethanol was added 20 mg of 10% palladium-carbon, and the mixture was stirred under hydrogen atmosphere at room temperature for 5 hours. The insoluble was removed by filtration, and the filtrate was concentrated under reduced pressure to give 82 mg of tert-butyl [2-(2-amino-4-isopropylphenyl)ethyl]carbamate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07022689B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-33df552e071d4bb5a29654b48748c713 |
| Source note | uspto-grants-2006_04 |