HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol hydrochloride → HCID 22219494, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol hydrochloride | HCID 21887872 | — |
| Reactant | HCID 86595213 | HCID 86595213 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22219494 | HCID 22219494 | — |
Reaction Steps
To a stirred solution of 0.266 g of ethyl [2-(2-tert-butoxycarbonylaminoethyl)-5-isopropylphenyl]oxalamate in 2 mL of ethanol was added 2 mL of 21% hydrogen chloride-ethanol solution at room temperature. After being stirred at the same temperature for 2 hours, the reaction mixture was concentrated under reduced pressure to give 0.179 g of ethyl N-[2-(2-aminoethyl)-5-isopropylphenyl]oxalamate hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07022689B2 |
| Source dataset | uspto-grants-2006_04 |
| ORD ID | ord-a2366e2f821b4357b4bad0d053c43fe0 |
| Source note | uspto-grants-2006_04 |