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HRID1794140

反应详情

EQUATION

反应方程式

HRID 1794140 的结构方程式

REACTANTS

反应物

3
结构：OCc1c(F)cccc1F
HCID87921

2,6-Difluorobenzyl alcohol

C7H6F2O

结构：CC[C@@H]1CN(C(=O)OC(C)(C)C)CCN1C(=O)OCc1c(F)cccc1F
HCID69143773

未命名化合物

结构：CC[C@@H]1CN(C(=O)OC(C)(C)C)CCN1C(=O)Cl
HCID86586001

未命名化合物

PRODUCTS

生成物

1
结构：CC[C@@H]1CNCCN1C(=O)OCc1c(F)cccc1F
HCID69142116

未命名化合物

PROCEDURE

实验过程

This compound was prepared from (R)-4-chlorocarbonyl-3-ethyl-piperazine-1-carboxylic acid tert-butyl ester and 2,6-difluorobenzylalcohol via (R)-2-ethyl-piperazine-1,4-dicarboxylic acid 4-tert-butyl ester 1-(2,6-difluoro-benzyl) ester according to the procedures described in Example 177 to give the product as a yellowish oil (69 mg); MS (ISP): 285.2 (M+H)+.